TA Instruments

AR1708-0001f

04/09/2012 16:43:13

Sample name	ASW 10 mm from base, 60 mm to top, disk 7 PMMA fouled AND CLEANED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1708
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:43:13

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-37.65	5.873	-6.411	1.0000	22.4	493.5	2.1485	10000	0.1211	14.31	2.6857	268.57	3.384E-3	0.0	1.0	61.000	-115.51	4.698
0.7782	12.66	0.06146	2.0040	22.4	505.9	13.7069	10000	0.1242	3.155	17.134	1713.4	3.384E-3	0.0	1.0	62.004	2.3876	10.13
1.532	19.54	0.07842	3.0080	22.4	502.6	27.3638	10000	0.1234	1.316	34.205	3420.5	3.384E-3	0.1	1.1	63.008	4.7017	15.63
2.108	23.19	0.09092	4.0040	22.4	488.6	41.4022	10000	0.1199	0.9086	51.753	5175.3	3.384E-3	0.1	1.1	64.004	6.4683	18.55
3.394	30.95	0.1097	5.0040	22.4	493.5	68.0236	10000	0.1211	0.5151	85.030	8503.0	3.383E-3	0.1	1.1	65.004	10.412	24.76
5.160	39.57	0.1304	6.0040	22.4	505.1	107.1160	10000	0.1240	0.3226	133.90	13390	3.384E-3	0.1	1.1	66.004	15.831	31.66
5.884	42.61	0.1381	7.0040	22.4	503.4	126.7610	10000	0.1236	0.2772	158.45	15845	3.383E-3	0.1	1.1	67.004	18.051	34.09
7.487	49.20	0.1522	8.0040	22.4	496.0	165.9450	10000	0.1217	0.2049	207.43	20743	3.384E-3	0.1	1.1	68.004	22.969	39.36
9.812	57.60	0.1704	9.0040	22.4	504.3	223.9800	10000	0.1238	0.1520	279.98	27998	3.384E-3	0.2	1.2	69.004	30.103	46.08
11.76	63.74	0.1844	10.004	22.4	499.3	275.1050	10000	0.1225	0.1229	343.88	34388	3.384E-3	0.2	1.2	70.004	36.068	50.99
13.69	69.70	0.1964	11.004	22.4	491.0	326.4440	10000	0.1205	0.1011	408.06	40806	3.384E-3	0.2	1.2	71.004	41.999	55.76
15.56	75.16	0.2070	12.004	22.4	479.5	377.8790	10000	0.1177	0.08487	472.35	47235	3.384E-3	0.2	1.2	72.004	47.724	60.13
17.42	80.55	0.2163	13.004	22.4	470.4	435.4030	10000	0.1154	0.07249	544.25	54425	3.384E-3	0.2	1.2	73.004	53.452	64.44
19.70	86.46	0.2278	14.008	22.4	474.5	499.0010	10000	0.1165	0.06347	623.75	62375	3.383E-3	0.2	1.2	74.008	60.431	69.17
22.59	94.63	0.2387	15.004	22.4	472.8	594.6550	10000	0.1161	0.05280	743.32	74332	3.384E-3	0.3	1.3	75.004	69.303	75.71
24.79	99.94	0.2481	16.004	22.4	465.4	664.5620	10000	0.1142	0.04660	830.70	83070	3.384E-3	0.3	1.3	76.004	76.054	79.95
26.82	105.7	0.2538	16.996	22.4	443.1	740.9140	10000	0.1088	0.03967	926.14	92614	3.384E-3	0.3	1.3	76.996	82.284	84.55
30.12	113.8	0.2648	18.000	22.4	466.2	855.6930	10000	0.1144	0.03603	1069.6	1.0696E5	3.384E-3	0.3	1.3	78.000	92.414	91.00
32.71	118.8	0.2753	19.000	22.4	457.1	931.9860	10000	0.1122	0.03238	1165.0	1.1650E5	3.384E-3	0.3	1.3	79.000	100.36	95.05
34.84	124.3	0.2804	20.004	22.4	446.4	1021.0500	10000	0.1096	0.02891	1276.3	1.2763E5	3.384E-3	0.3	1.3	80.004	106.89	99.41
38.82	132.3	0.2934	21.004	22.4	461.3	1153.6400	10000	0.1132	0.02635	1442.1	1.4421E5	3.384E-3	0.4	1.4	81.004	119.11	105.8
40.84	137.4	0.2972	22.004	22.4	462.9	1242.4200	10000	0.1136	0.02452	1553.0	1.5530E5	3.384E-3	0.4	1.4	82.004	125.29	109.9
43.88	142.8	0.3072	23.000	22.4	454.7	1344.1100	10000	0.1116	0.02229	1680.1	1.6801E5	3.384E-3	0.4	1.4	83.000	134.61	114.3
47.93	150.8	0.3178	24.004	22.4	445.6	1495.9000	10000	0.1094	0.01959	1869.9	1.8699E5	3.384E-3	0.4	1.4	84.004	147.03	120.7
50.58	155.9	0.3243	25.004	22.4	437.3	1597.2800	10000	0.1073	0.01798	1996.6	1.9966E5	3.383E-3	0.4	1.4	85.004	155.17	124.7
53.28	161.3	0.3302	26.004	22.4	449.7	1711.3300	10000	0.1104	0.01728	2139.2	2.1392E5	3.384E-3	0.4	1.4	86.004	163.45	129.1
57.67	169.3	0.3406	27.004	22.4	441.4	1882.2100	10000	0.1083	0.01539	2352.8	2.3528E5	3.384E-3	0.5	1.5	87.004	176.94	135.5
60.48	174.5	0.3467	28.004	22.4	433.2	1996.1801	10000	0.1063	0.01423	2495.2	2.4952E5	3.383E-3	0.5	1.5	88.004	185.55	139.6
63.19	179.6	0.3519	29.000	22.4	434.0	2116.3301	10000	0.1065	0.01346	2645.4	2.6454E5	3.384E-3	0.5	1.5	89.000	193.86	143.7
67.40	187.6	0.3593	30.000	22.4	420.8	2306.8999	10000	0.1033	0.01196	2883.6	2.8836E5	3.384E-3	0.5	1.5	90.000	206.77	150.1
70.94	192.7	0.3681	31.004	22.4	412.5	2432.7400	10000	0.1012	0.01111	3040.9	3.0409E5	3.384E-3	0.5	1.5	91.004	217.66	154.2
74.02	197.8	0.3741	32.000	22.4	410.0	2565.4099	10000	0.1006	0.01048	3206.8	3.2068E5	3.384E-3	0.5	1.5	92.000	227.09	158.3
78.75	205.8	0.3826	33.000	22.4	414.2	2775.3401	10000	0.1016	9.775E-3	3469.2	3.4692E5	3.384E-3	0.6	1.6	93.000	241.62	164.7
82.19	211.0	0.3895	34.004	22.4	400.1	2914.7900	10000	0.09820	8.987E-3	3643.5	3.6435E5	3.383E-3	0.6	1.6	94.004	252.15	168.8
86.24	218.6	0.3945	34.996	22.4	411.7	3128.2600	10000	0.1010	8.614E-3	3910.3	3.9103E5	3.384E-3	0.6	1.6	94.996	264.58	174.9
89.95	223.9	0.4017	36.000	22.4	405.9	3279.5701	10000	0.09962	8.096E-3	4099.5	4.0995E5	3.384E-3	0.6	1.6	96.000	275.95	179.1
95.22	229.1	0.4156	37.008	22.4	390.2	3431.1001	10000	0.09576	7.435E-3	4288.9	4.2889E5	3.384E-3	0.6	1.6	97.008	292.12	183.3
99.17	236.6	0.4191	37.996	22.4	384.4	3659.1699	10000	0.09434	6.864E-3	4574.0	4.5740E5	3.383E-3	0.6	1.6	97.996	304.24	189.3
101.7	241.8	0.4206	39.004	22.4	390.2	3823.4299	10000	0.09576	6.671E-3	4779.3	4.7793E5	3.384E-3	0.7	1.7	99.004	312.08	193.5
107.6	249.6	0.4310	39.996	22.4	376.1	4071.2000	10000	0.09232	6.038E-3	5089.0	5.0890E5	3.383E-3	0.7	1.7	99.996	330.00	199.7
110.2	254.6	0.4329	41.000	22.4	380.3	4233.8501	10000	0.09333	5.865E-3	5292.3	5.2923E5	3.384E-3	0.7	1.7	101.000	338.16	203.7
115.3	259.8	0.4436	42.000	22.4	392.7	4501.5000	10000	0.09637	5.816E-3	5626.9	5.6269E5	3.384E-3	0.7	1.7	102.000	353.66	207.9
119.3	267.6	0.4459	43.000	22.4	393.5	4674.7402	10000	0.09658	5.494E-3	5843.4	5.8434E5	3.384E-3	0.7	1.7	103.000	366.14	214.1
123.7	272.7	0.4536	44.000	22.4	367.0	4853.0801	10000	0.09008	4.936E-3	6066.4	6.0664E5	3.384E-3	0.7	1.7	104.000	379.50	218.1
129.3	280.4	0.4613	45.004	22.4	362.1	5130.5898	10000	0.08887	4.607E-3	6413.2	6.4132E5	3.384E-3	0.8	1.8	105.004	396.78	224.3
134.0	285.5	0.4692	46.000	22.4	351.3	5318.5601	10000	0.08623	4.309E-3	6648.2	6.6482E5	3.383E-3	0.8	1.8	106.000	411.04	228.4
139.6	293.1	0.4763	47.000	22.4	355.5	5602.4302	10000	0.08724	4.137E-3	7003.0	7.0030E5	3.384E-3	0.8	1.8	107.000	428.30	234.5
142.8	298.1	0.4790	48.004	22.4	336.4	5798.0000	10000	0.08258	3.785E-3	7247.5	7.2475E5	3.384E-3	0.8	1.8	108.004	438.17	238.5
147.6	303.3	0.4867	49.000	22.4	324.0	6001.5801	10000	0.07953	3.522E-3	7502.0	7.5020E5	3.384E-3	0.8	1.8	109.000	452.94	242.7
152.1	311.0	0.4892	49.996	22.4	324.9	6302.5098	10000	0.07974	3.360E-3	7878.1	7.8781E5	3.383E-3	0.8	1.8	109.996	466.68	248.8
157.4	316.0	0.4981	51.016	22.4	321.6	6510.8999	10000	0.07892	3.220E-3	8138.6	8.1386E5	3.384E-3	0.9	1.9	111.016	482.93	252.8
161.6	323.8	0.4991	52.004	22.4	332.3	6832.5098	10000	0.08156	3.169E-3	8540.6	8.5406E5	3.384E-3	0.9	1.9	112.004	495.80	259.0
167.3	328.9	0.5088	53.004	22.4	306.7	7046.7900	10000	0.07527	2.835E-3	8808.5	8.8085E5	3.384E-3	0.9	1.9	113.004	513.36	263.1
173.6	336.4	0.5159	54.012	22.4	281.9	7376.7402	10000	0.06919	2.491E-3	9220.9	9.2209E5	3.384E-3	0.9	1.9	114.012	532.46	269.1
178.3	341.6	0.5221	55.004	22.4	289.3	7602.4702	10000	0.07101	2.479E-3	9503.1	9.5031E5	3.384E-3	0.9	1.9	115.004	547.12	273.3
182.4	346.7	0.5262	56.000	22.4	293.5	7828.8599	10000	0.07203	2.441E-3	9786.1	9.7861E5	3.384E-3	0.9	1.9	116.000	559.73	277.4
189.9	354.2	0.5360	57.016	22.4	312.5	8171.0601	10000	0.07669	2.490E-3	10214	1.0214E6	3.384E-3	1.0	2.0	117.016	582.53	283.4
193.2	359.3	0.5376	58.000	22.4	297.6	8408.7002	10000	0.07304	2.305E-3	10511	1.0511E6	3.383E-3	1.0	2.0	118.000	592.65	287.5
201.1	367.0	0.5480	59.004	22.4	286.0	8768.0498	10000	0.07020	2.124E-3	10960	1.0960E6	3.384E-3	1.0	2.0	119.004	617.04	293.6
205.7	372.0	0.5530	60.012	22.4	281.1	9007.8096	10000	0.06898	2.031E-3	11260	1.1260E6	3.384E-3	1.0	2.0	120.012	631.09	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

208.6	375.0	0.5562	0.99600	22.4	309.2	280.8380	10000	0.07588	2.198E-3	351.05	35105	3.383E-3	0.0	2.0	121.996	639.89	300.0
210.6	375.0	0.5615	2.0120	22.4	275.3	532.3130	10000	0.06756	1.957E-3	665.39	66539	3.383E-3	0.0	2.1	123.012	646.00	300.0
211.2	375.0	0.5631	3.0000	22.4	259.6	909.0350	10000	0.06371	1.846E-3	1136.3	1.1363E5	3.384E-3	0.1	2.1	124.000	647.85	300.0
208.9	375.0	0.5571	3.9960	22.4	265.4	1160.5500	10000	0.06513	1.887E-3	1450.7	1.4507E5	3.383E-3	0.1	2.1	124.996	640.87	300.0
206.4	375.0	0.5504	5.0120	22.4	326.5	1413.3300	10000	0.08014	2.322E-3	1766.7	1.7667E5	3.384E-3	0.1	2.1	126.012	633.23	300.0
206.9	375.0	0.5517	6.0120	22.4	275.3	1790.3800	10000	0.06756	1.957E-3	2238.0	2.2380E5	3.384E-3	0.1	2.1	127.012	634.75	300.0
208.1	375.0	0.5549	7.0120	22.4	264.5	2042.3600	10000	0.06493	1.881E-3	2553.0	2.5530E5	3.384E-3	0.1	2.1	128.012	638.45	300.0
208.8	375.0	0.5567	8.0080	22.4	257.9	2418.6001	10000	0.06330	1.834E-3	3023.3	3.0233E5	3.384E-3	0.1	2.2	129.008	640.51	300.0
209.1	375.0	0.5575	8.9960	22.4	273.6	2668.4099	10000	0.06716	1.946E-3	3335.5	3.3355E5	3.384E-3	0.1	2.2	129.996	641.38	300.0
212.2	375.0	0.5658	9.9960	22.4	240.6	2919.7200	10000	0.05904	1.711E-3	3649.7	3.6497E5	3.384E-3	0.2	2.2	130.996	650.89	300.0
209.4	375.0	0.5584	11.016	22.4	248.8	3296.8000	10000	0.06107	1.769E-3	4121.0	4.1210E5	3.384E-3	0.2	2.2	132.016	642.47	300.0
207.7	375.0	0.5539	12.012	22.4	275.3	3547.9800	10000	0.06756	1.957E-3	4435.0	4.4350E5	3.384E-3	0.2	2.2	133.012	637.28	300.0
211.4	375.0	0.5638	13.012	22.4	296.8	3926.4099	10000	0.07284	2.110E-3	4908.0	4.9080E5	3.384E-3	0.2	2.2	134.012	648.62	300.0
208.2	375.0	0.5552	14.012	22.4	309.2	4181.2402	10000	0.07588	2.198E-3	5226.6	5.2266E5	3.384E-3	0.2	2.3	135.012	638.79	300.0
208.6	375.0	0.5562	15.000	22.4	256.3	4427.7998	10000	0.06290	1.822E-3	5534.8	5.5348E5	3.384E-3	0.3	2.3	136.000	639.97	300.0
209.3	375.0	0.5581	16.012	22.4	279.4	4804.7202	10000	0.06858	1.987E-3	6005.9	6.0059E5	3.383E-3	0.3	2.3	137.012	642.05	300.0
208.7	375.0	0.5564	17.020	22.4	297.6	5057.6201	10000	0.07304	2.116E-3	6322.0	6.3220E5	3.384E-3	0.3	2.3	138.020	640.16	300.0
210.4	375.0	0.5610	18.012	22.4	261.2	5307.3901	10000	0.06411	1.858E-3	6634.2	6.6342E5	3.384E-3	0.3	2.3	139.012	645.40	300.0
209.3	375.0	0.5581	19.012	22.4	266.2	5684.2100	10000	0.06533	1.893E-3	7105.3	7.1053E5	3.384E-3	0.3	2.3	140.012	642.09	300.0
210.1	375.0	0.5604	20.012	22.4	280.2	5935.7300	10000	0.06878	1.993E-3	7419.7	7.4197E5	3.384E-3	0.3	2.4	141.012	644.71	300.0
207.7	375.0	0.5540	21.016	22.4	255.4	6312.8599	10000	0.06269	1.816E-3	7891.1	7.8911E5	3.384E-3	0.4	2.4	142.016	637.33	300.0
209.2	375.0	0.5579	22.012	22.4	256.3	6564.0098	10000	0.06290	1.822E-3	8205.0	8.2050E5	3.384E-3	0.4	2.4	143.012	641.85	300.0
205.5	375.0	0.5479	23.012	22.4	266.2	6815.2300	10000	0.06533	1.893E-3	8519.0	8.5190E5	3.384E-3	0.4	2.4	144.012	630.42	300.0
209.1	375.0	0.5575	24.012	22.4	238.9	7192.2500	10000	0.05864	1.699E-3	8990.3	8.9903E5	3.384E-3	0.4	2.4	145.012	641.41	300.0
211.2	375.0	0.5632	25.012	22.4	268.7	7443.8901	10000	0.06594	1.911E-3	9304.9	9.3049E5	3.384E-3	0.4	2.4	146.012	647.97	300.0
206.8	375.0	0.5514	26.020	22.4	322.4	7823.0200	10000	0.07913	2.293E-3	9778.8	9.7788E5	3.383E-3	0.4	2.5	147.020	634.40	300.0
208.3	375.0	0.5555	27.016	22.4	259.6	8071.8301	10000	0.06371	1.846E-3	10090	1.0090E6	3.383E-3	0.5	2.5	148.016	639.15	300.0
206.8	375.0	0.5514	28.012	22.4	271.1	8323.2900	10000	0.06655	1.928E-3	10404	1.0404E6	3.384E-3	0.5	2.5	149.012	634.42	300.0
209.3	375.0	0.5581	29.016	22.4	237.2	8700.2998	10000	0.05823	1.687E-3	10875	1.0875E6	3.384E-3	0.5	2.5	150.016	642.14	300.0
211.3	375.0	0.5635	30.012	22.4	273.6	8951.6797	10000	0.06716	1.946E-3	11190	1.1190E6	3.384E-3	0.5	2.5	151.012	648.26	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

205.3	370.0	0.5549	1.0160	22.4	240.6	317.3470	10000	0.05904	1.757E-3	396.68	39668	3.383E-3	0.0	2.5	152.016	629.95	296.0
202.4	365.0	0.5545	2.0160	22.4	282.7	555.1410	10000	0.06939	2.122E-3	693.93	69393	3.384E-3	0.0	2.6	153.016	621.01	292.0
196.1	360.0	0.5447	3.0120	22.4	240.6	793.2020	10000	0.05904	1.857E-3	991.50	99150	3.383E-3	0.1	2.6	154.012	601.56	288.0
188.2	352.3	0.5343	4.0120	22.4	306.7	1144.4000	10000	0.07527	2.471E-3	1430.5	1.4305E5	3.384E-3	0.1	2.6	155.012	577.44	281.8
182.8	347.3	0.5265	5.0160	22.4	300.9	1369.2800	10000	0.07385	2.495E-3	1711.6	1.7116E5	3.384E-3	0.1	2.6	156.016	560.95	277.8
177.0	339.7	0.5209	6.0200	22.4	283.5	1707.3700	10000	0.06959	2.457E-3	2134.2	2.1342E5	3.384E-3	0.1	2.6	157.020	542.90	271.7
174.3	334.5	0.5212	7.0120	22.4	253.0	1936.8400	10000	0.06208	2.261E-3	2421.1	2.4211E5	3.383E-3	0.1	2.6	158.012	534.83	267.6
166.6	327.0	0.5096	8.0160	22.4	332.3	2252.0200	10000	0.08156	3.108E-3	2815.0	2.8150E5	3.383E-3	0.1	2.7	159.016	511.23	261.6
162.6	321.9	0.5052	9.0120	22.4	325.7	2466.2900	10000	0.07994	3.143E-3	3082.9	3.0829E5	3.383E-3	0.2	2.7	160.012	498.91	257.5
157.8	316.7	0.4983	10.012	22.4	334.0	2677.6101	10000	0.08197	3.329E-3	3347.0	3.3470E5	3.384E-3	0.2	2.7	161.012	484.26	253.4
151.9	309.1	0.4915	11.020	22.4	325.7	2984.4600	10000	0.07994	3.409E-3	3730.6	3.7306E5	3.384E-3	0.2	2.7	162.020	466.06	247.3
148.9	304.0	0.4898	12.012	22.4	329.8	3184.6001	10000	0.08095	3.568E-3	3980.8	3.9808E5	3.384E-3	0.2	2.7	163.012	456.86	243.2
143.8	296.3	0.4853	13.016	22.4	316.6	3484.9900	10000	0.07771	3.607E-3	4356.2	4.3562E5	3.384E-3	0.2	2.7	164.016	441.12	237.0
138.9	291.1	0.4772	14.012	22.4	343.9	3678.9500	10000	0.08440	4.059E-3	4598.7	4.5987E5	3.384E-3	0.2	2.8	165.012	426.11	232.9
131.6	283.5	0.4640	15.016	22.4	367.9	3960.6201	10000	0.09029	4.577E-3	4950.8	4.9508E5	3.383E-3	0.3	2.8	166.016	403.62	226.8
128.6	278.3	0.4619	16.020	22.4	354.6	4148.1401	10000	0.08704	4.577E-3	5185.2	5.1852E5	3.384E-3	0.3	2.8	167.020	394.41	222.7
124.1	273.2	0.4541	17.008	22.4	371.2	4329.6699	10000	0.09110	4.974E-3	5412.1	5.4121E5	3.384E-3	0.3	2.8	168.008	380.61	218.5
117.9	265.6	0.4437	18.012	22.4	394.3	4592.2598	10000	0.09678	5.588E-3	5740.3	5.7403E5	3.384E-3	0.3	2.8	169.012	361.59	212.5
116.7	260.5	0.4481	19.012	22.4	368.7	4767.3398	10000	0.09049	5.434E-3	5959.2	5.9592E5	3.384E-3	0.3	2.8	170.012	358.12	208.4
109.4	252.7	0.4330	20.012	22.4	376.1	5023.7100	10000	0.09232	5.892E-3	6279.6	6.2796E5	3.384E-3	0.3	2.9	171.012	335.62	202.1
106.0	247.6	0.4282	21.020	22.4	369.5	5186.3198	10000	0.09069	6.026E-3	6482.9	6.4829E5	3.384E-3	0.4	2.9	172.020	325.30	198.1
101.5	242.5	0.4185	22.012	22.4	397.6	5349.0098	10000	0.09759	6.762E-3	6686.3	6.6863E5	3.384E-3	0.4	2.9	173.012	311.35	194.0
96.68	234.6	0.4121	23.012	22.4	386.0	5592.6099	10000	0.09475	7.015E-3	6990.8	6.9908E5	3.384E-3	0.4	2.9	174.012	296.60	187.7
92.95	229.5	0.4050	24.012	22.4	393.5	5742.6602	10000	0.09658	7.472E-3	7178.3	7.1783E5	3.384E-3	0.4	2.9	175.012	285.16	183.6
88.58	221.8	0.3994	25.016	22.4	416.6	5968.3999	10000	0.1023	8.471E-3	7460.5	7.4605E5	3.384E-3	0.4	2.9	176.016	271.75	177.4
85.96	216.5	0.3971	26.020	22.4	391.8	6117.7402	10000	0.09617	8.362E-3	7647.2	7.6472E5	3.384E-3	0.4	3.0	177.020	263.71	173.2
81.41	211.4	0.3851	27.012	22.4	401.8	6255.0498	10000	0.09860	8.990E-3	7818.8	7.8188E5	3.384E-3	0.5	3.0	178.012	249.78	169.1
76.74	203.7	0.3767	28.012	22.4	421.6	6461.1099	10000	0.1035	0.01016	8076.4	8.0764E5	3.384E-3	0.5	3.0	179.012	235.44	163.0
73.78	198.4	0.3719	29.016	22.4	423.2	6599.2002	10000	0.1039	0.01075	8249.0	8.2490E5	3.384E-3	0.5	3.0	180.016	226.37	158.7
69.39	193.1	0.3593	29.996	22.4	414.2	6793.0400	10000	0.1016	0.01111	8491.3	8.4913E5	3.384E-3	0.5	3.0	180.996	212.90	154.5
65.72	185.5	0.3543	31.020	22.4	418.3	6916.9702	10000	0.1027	0.01216	8646.2	8.6462E5	3.384E-3	0.5	3.0	182.020	201.62	148.4
63.04	180.2	0.3499	32.012	22.4	421.6	7041.7202	10000	0.1035	0.01299	8802.2	8.8022E5	3.384E-3	0.5	3.1	183.012	193.42	144.1
58.40	172.4	0.3388	33.012	22.4	424.1	7216.3999	10000	0.1041	0.01427	9020.5	9.0205E5	3.384E-3	0.6	3.1	184.012	179.17	137.9
56.12	167.3	0.3355	34.020	22.4	440.6	7329.8101	10000	0.1081	0.01575	9162.3	9.1623E5	3.384E-3	0.6	3.1	185.020	172.16	133.8
53.91	162.0	0.3328	35.012	22.4	431.5	7441.0298	10000	0.1059	0.01645	9301.3	9.3013E5	3.384E-3	0.6	3.1	186.012	165.40	129.6
48.40	153.9	0.3145	35.996	22.4	463.8	7603.0801	10000	0.1138	0.01958	9503.9	9.5039E5	3.384E-3	0.6	3.1	186.996	148.48	123.1
45.69	148.8	0.3071	37.012	22.4	454.7	7702.8301	10000	0.1116	0.02053	9628.5	9.6285E5	3.383E-3	0.6	3.1	188.012	140.19	119.0
43.36	143.5	0.3021	38.016	22.4	463.8	7802.3901	10000	0.1138	0.02251	9753.0	9.7530E5	3.384E-3	0.6	3.2	189.016	133.02	114.8
39.73	135.4	0.2934	39.012	22.4	467.1	7946.0898	10000	0.1146	0.02548	9932.6	9.9326E5	3.383E-3	0.7	3.2	190.012	121.88	108.3
37.38	130.3	0.2868	40.016	22.4	451.4	8032.8101	10000	0.1108	0.02657	10041	1.0041E6	3.384E-3	0.7	3.2	191.016	114.68	104.3
35.01	125.1	0.2800	41.024	22.4	454.7	8119.9199	10000	0.1116	0.02907	10150	1.0150E6	3.384E-3	0.7	3.2	192.024	107.41	100.0
30.92	116.7	0.2650	42.016	22.4	451.4	8250.8096	10000	0.1108	0.03314	10314	1.0314E6	3.384E-3	0.7	3.2	193.016	94.870	93.36
29.01	111.4	0.2603	43.016	22.4	469.5	8325.0098	10000	0.1152	0.03782	10406	1.0406E6	3.383E-3	0.7	3.2	194.016	88.989	89.14
26.54	106.1	0.2501	44.012	22.4	467.9	8399.5498	10000	0.1148	0.04155	10499	1.0499E6	3.383E-3	0.7	3.3	195.012	81.438	84.90
24.33	100.5	0.2420	45.012	22.4	472.0	8473.9805	10000	0.1159	0.04669	10592	1.0592E6	3.384E-3	0.8	3.3	196.012	74.653	80.44
21.06	92.34	0.2281	46.008	22.4	464.6	8573.1699	10000	0.1140	0.05449	10716	1.0716E6	3.383E-3	0.8	3.3	197.008	64.606	73.87
19.32	86.99	0.2221	47.012	22.4	469.5	8635.0996	10000	0.1152	0.06205	10794	1.0794E6	3.383E-3	0.8	3.3	198.012	59.266	69.59
17.48	81.30	0.2150	48.016	22.4	471.2	8696.8701	10000	0.1156	0.07129	10871	1.0871E6	3.383E-3	0.8	3.3	199.016	53.637	65.04
15.21	75.51	0.2014	49.016	22.4	475.3	8778.0898	10000	0.1167	0.08336	10973	1.0973E6	3.384E-3	0.8	3.3	200.016	46.656	60.41
12.84	67.49	0.1902	50.016	22.4	498.5	8826.5400	10000	0.1223	0.1094	11033	1.1033E6	3.384E-3	0.8	3.4	201.016	39.381	53.99
10.78	61.59	0.1751	51.020	22.4	479.5	8875.6699	10000	0.1177	0.1264	11095	1.1095E6	3.383E-3	0.9	3.4	202.020	33.076	49.27
8.951	55.51	0.1612	52.012	22.4	491.9	8918.6104	10000	0.1207	0.1596	11148	1.1148E6	3.384E-3	0.9	3.4	203.012	27.461	44.41
7.480	50.12	0.1492	53.012	22.4	484.4	8955.5703	10000	0.1189	0.1929	11194	1.1194E6	3.384E-3	0.9	3.4	204.012	22.948	40.09
6.168	44.10	0.1399	53.996	22.4	490.2	8991.8701	10000	0.1203	0.2521	11240	1.1240E6	3.384E-3	0.9	3.4	204.996	18.925	35.28
4.832	37.82	0.1278	55.016	22.4	490.2	9022.1504	10000	0.1203	0.3428	11278	1.1278E6	3.384E-3	0.9	3.4	206.016	14.824	30.25
3.685	32.47	0.1135	56.020	22.4	500.1	9046.3301	10000	0.1227	0.4744	11308	1.1308E6	3.384E-3	0.9	3.5	207.020	11.307	25.97
2.530	26.14	0.09678	57.012	22.4	497.6	9070.0703	10000	0.1221	0.7282	11338	1.1338E6	3.384E-3	1.0	3.5	208.012	7.7621	20.91
1.951	22.39	0.08714	58.012	22.4	500.1	9081.6299	10000	0.1227	0.9974	11352	1.1352E6	3.384E-3	1.0	3.5	209.012	5.9862	17.91
0.9401	14.04	0.06697	59.016	22.4	501.0	9098.4199	10000	0.1230	2.542	11373	1.1373E6	3.383E-3	1.0	3.5	210.016	2.8841	11.23
0.3018	7.089	0.04257	60.012	22.4	492.7	9106.3799	10000	0.1209	9.803	11383	1.1383E6	3.384E-3	1.0	3.5	211.012	0.92589	5.671

